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Lichrosolv® Prepsolv®液相色谱溶剂

液相色谱法已经成为研发、药物质量控制和环境分析领域的关键手段。因而对所使用的溶剂也有很高的要求。
HPLC溶剂具备低紫外吸收，低悬浮颗粒，低酸碱度和低蒸发残留的优点，经过严格的原材料选取，从开始投料生产到后期包装出厂多次进行过纯化。
LC/MS的Lichrosolv® 产品可以达成现代LC/MS离子化方法对准确检测的要求。且其包装材料也经过LC/MS质量要求的测试。
为了使分析到制备分离变得容易，Prepsolv®溶剂能够适合制备液相的要求。它们具有很低的蒸发残留（<1mg/l）和含水量，并在惰性气体下灌装。

描述
产品目录编号	106007
同义词	MeOH, Hydroxymethane, Methyl alcohol, Carbinol
概述	With their high degree of UV transmittance, low particle count, low acidity and alkalinity and low evaporation residue level, LiChrosolv® solvents are ideal for reproducible separations. Since separations are normally carried out under gradient conditions in analytical HPLC, we offer solvents in "gradient grade" as well as "isocratic grade". This enables to minimize the gradient effect of the solvent involved.

产品信息
CAS号	67-56-1
EC索引编号	603-001-00-X
EC号	200-659-6
级别	Reag. Ph Eur
Hill配方	CH₄O
化学配方	CH₃OH
Molar Mass	32.04 g/mol
HS代码	2905 11 00
结构配方图像

应用
应用	Methanol gradient grade for liquid chromatography LiChrosolv® Reag. Ph Eur. CAS 67-56-1, chemical formula CH₃OH, molar mass 32.04 g/mol.

理化信息
沸点	64.5 °C (1013 hPa)
密度	0.792 g/cm3 (20 °C)
汽化值	1.9
爆炸极限	5.5 - 44 %(V)
闪点	10 °C
燃点	455 °C DIN 51794
熔点	-98 °C
蒸汽压力	128 hPa (20 °C)

毒性学信息
LD 50口服	LD50 Rat 5628 mg/kg
LD 50皮下注射	LD50 Rabbit 17100 mg/kg

GHS安全信息
危害性图示
危害性声明	H225: 高度易燃液体和蒸气。 H301 + H311 + H331: 吞咽、皮肤接触或吸入可致中毒。 H370: 会损害器官。
注意事项声明	P210: 远离热源、热表面、火花、明火和其他点火源。禁止吸烟。 P240: 容器和接收设备接地、连接。 P280: 戴防护手套/穿防护服。 P302 + P352: 如果皮肤接触：用大量肥皂和水清洗。 P304 + P340: 如误吸入：将患者转移到空气新鲜处，保持呼吸舒适的休息姿势。 P308 + P310: 如有接触或有疑虑：立即呼叫中毒控制中心或就医。 P403 + P233: 存放在通风良好的地方。保持容器密闭。
RTECS	PC1400000
储存类别	3 易燃液体
WGK	WGK 1 轻度的水危害
一次性	1 有机无卤素溶剂: Category A.

安全信息
危害性符号	Flammable Toxic
危险种类	?????, ???
R相	R 11-23/24/25-39/23/24/25 Highly flammable.Toxic by inhalation, in contact with skin and if swallowed.Toxic: danger of very serious irreversible effects through inhalation, in contact with skin and if swallowed.
S相	S 7-16-36/37-45 Keep container tightly closed.Keep away from sources of ignition - No smoking.Wear suitable protective clothing and gloves.In case of accident or if you feel unwell, seek medical advice immediately (show the label where possible).

储存和货运信息
储存	于 +5°C 到 +30°C储存.

运输信息
申报（铁路和陆路）ADR、RID	UN 1230 , 3 (6.1), II
申报（空运）IATA-DGR	UN 1230 , 3 (6.1), II
申报（海运）IMDG-代码	UN 1230 , 3 (6.1), II

规格
Purity (GC)	≥ 99.9 %
Identity (IR)	conforms
Evaporation residue	≤ 2.0 mg/l
Water	≤ 0.02 %
Colour	≤ 10 Hazen
Density (d 20 °C/20 °C)	0.791 - 0.793
Boiling point	64 - 65 °C
Acidity	≤ 0.0002 meq/g
Alkalinity	≤ 0.0002 meq/g
Gradient grade (at 235 nm)	≤ 2.0 mAU
Gradient grade (at 254 nm)	≤ 1.0 mAU
Fluorescence (as quinine at 254 nm)	≤ 1.0 ppb
Fluorescence (as quinine at 365 nm)	≤ 0.5 ppb
Transmission (at 210 nm)	≥ 20 %
Transmission (at 220 nm)	≥ 60 %
Transmission (at 230 nm)	≥ 75 %
Transmission (at 235 nm)	≥ 83 %
Transmission (at 250 nm)	≥ 95 %
Transmission (from 260 nm)	≥ 98 %
Absorbance (at 225 nm)	≤ 0.170
Filtered by 0.2 µm filter. Suitable for UPLC / UHPLC /Ultra HPLC - instruments. Conforms to Methanol R1 and R2 according to Reag. Ph Eur; conforms to the requirements of ACS for liquid chromatography suitability.

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HPLC甲醇